Surface water quality deterioration due to industrial and agricultural processes is severe in Bangladesh, especially where the industrial and agricultural activities go side by side in and around the surface water systems. The present environmental research work has been carried out during pre-monsoon and post-monsoon period of 2009 to evaluate the environmental impacts of agro-industrial processes on the adjoining surface water systems in the southeastern outskirt of Dhaka City. Twenty composite water samples were collected from different water sources of the vast study area following standard sampling techniques. The major physical-chemical parameters were determined using advanced analytical techniques. The water quality parameters evaluated were Temperature,